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- ItemGeoarchaeological studies on Roman time harbour sediments in Cologne — comparison of different OSL dating techniques(Warsaw : De Gruyter, 2011) Lauer, Tobias; Bonn, Rainer; Frechen, Manfred; Fuchs, Magret; Trier, Marcus; Tsukamoto, SumikoDue to the construction of a new North-South subway in Cologne, Roman time harbour sediments were exposed and were sampled for luminescence dating. A very good independent age control was given by the precise knowledge of the chronology of Roman activity and by radiocarbon ages of charcoal samples. Hence, different methodological approaches within luminescence dating were applied for Holocene heterogeneously bleached fluvial samples and were compared to the known ages. For one sample, optically stimulated luminescence (OSL) dating was applied to coarse-grained quartz using a single aliquot regenerative-dose (SAR) protocol. After De-measurements, dif-ferent statistical approaches were tested (i.e. arithmetic mean, median, minimum age model, finite mixture model, leading edge method and the Fuchs and Lang approach). It is demonstrated that the Fuchs and Lang approach along with the leading edge method yielded the best matching OSL ages with respect to the known ages. For the other sample which showed feldspar contamination within the quartz signal, the post-IR blue stimulated luminescence (double SAR protocol) was measured in three different ways to calculate the De-value: with continuous wave (CW) stimulation with an IR-bleach at 50°C and at 225°C for 100 s prior to the OSL, and pulsed OSL (POSL). It was demonstrated that the IR-stimulation at 225°C has very good potential to remove the feldspar signal contribution as well as pulsed OSL, but the former might deplete parts of the quartz OSL signal. © 2011 Silesian University of Technology, Gliwice, Poland. All rights reserved.
- ItemLuminescence Dating of Fluvial Deposits from the Weser Valley, Germany(Warsaw : De Gruyter, 2015) Roskosch, Julia; Tsukamoto, Sumiko; Frechen, ManfredLuminescence dating was applied on coarse-grained monomineralic potassium-rich feld-spar and polymineralic fine-grained minerals of five samples derived from fluvial deposits of the Riv-er Weser in northwestern Germany. We used a pulsed infrared stimulated luminescence (IRSL) single aliquot regenerative (SAR) dose protocol with an IR stimulation at 50°C for 400 s (50 μs on-time and 200 μs off-time). In order to obtain a stable luminescence signal, only off-time IRSL signal was rec-orded. Performance tests gave solid results. Anomalous fading was intended to be reduced by using the pulsed IRSL signal measured at 50°C (IR50), but fading correction was in most cases necessary due to moderate fading rates. Fading uncorrected and corrected pulsed IR50 ages revealed two major fluvial aggradation phases during the Late Pleistocene, namely during marine isotope stage (MIS) 5d (100 ± 5 ka) and from late MIS 5b to MIS 4 (77 ± 6 ka to 68 ± 5 ka). The obtained luminescence ages are consistent with previous 230Th/U dating results from underlying interglacial deposits of the same pit, which are correlated with MIS 7c to early MIS 6.
- ItemQuartz OSL and K-feldspar post-IR IRSL dating of sand accumulation in the Lower Liao Plain (Liaoning, NE China)(Warsaw : De Gruyter, 2017) Li, Yan; Tsukamoto, Sumiko; Hu, Ke; Frechen, ManfredThe timing of the formation of extensively distributed sand dunes in the Bohai coastal area and its forcing factors are poorly understood. In this study, the chronology of a well-preserved sand dune located in Panjin Forest Park (PJ) in the Lower Liao Plain (LLP) is investigated using quartz optically stimulated luminescence (OSL) and K-feldspar postinfrared (IR) infrared stimulated luminescence (IRSL) (pIRIR) dating. For the pIRIR measurements, the combination of preheating at 180°C and pIRIR stimulation at 150°C (pIRIR150) is exploited. The quartz results show that the sand dune accumulated from c. 120 a (1890 AD) to c. 70 a (1940 AD) before present, and the underlying sandy soil sediments deposited from c. 5.0 ka to c. 0.13 ka as marsh sediment after the sea level highstand since the mid-Holocene. From the evidence in historical coastline records, the PJ sand dune is an inland sand dune and not a coastal sand dune. Based on further information of climate and temperature change after the Little Ice Age (LIA) and human activity in northeastern China, we conclude that the PJ sand dune accumulation was very likely impacted by the immigrants and land reclamation at the end of Qing dynasty. The fading corrected IR50 ages, the apparent and fading corrected pIRIR150 ages are consistent with quartz ages for two sandy soil samples but overestimate those for six sand samples. The overestimation of the feldspar ages is derived from the residual signal which has not been bleached before burial. The offset obtained from the difference between the quartz OSL and the feldspar pIRIR150 ages are ~20-160 a (predicted residual dose: ~0.08-0.60 Gy), whereas the measured residual dose after bleaching 4 h in a solar simulator yielded age overestimation of ~10-40 a (~0.05-0.16 Gy). The age discrepancy calculated from the predicted residual was larger than those obtained from the laboratory measured residuals. We conclude that the pIRIR150 of aeolian sediment is applicable for samples older than ~1000 years where the effect of the residual dose become negligible. © 2016 Y. Li et al.
- ItemInfrared radiofluorescence (IR-RF) dating of middle pleistocene fluvial archives of the Heidelberg Basin (Southwest Germany)(Warsaw : De Gruyter, 2011) Lauer, Tobias; Krbetschek, Matthias; Frechen, Manfred; Tsukamoto, Sumiko; Hoselmann, Christian; Weidenfeller, MichaelThe infrared radiofluorescence (IR-RF) dating technique was applied to eight fluvial samples that were collected from two sediment cores at the Heidelberg Basin located near Viernheim and Ludwigshafen in southwest Germany. Based on the IR-RF derived ages of the samples it was possible to establish a chronological framework for the Mid-Pleistocene fluvial deposits of the Heidelberg Basin. The results allow us to distinguish between four main periods of aggradation. The lowermost sample taken from 100 m core depth lead to an IR-RF age of 643 ± 28 ka pointing to a Cromerian period of aggradation (OIS 17-16). For the Elsterian it is now possible to distinguish between two aggradation periods, one occurring during the Lower Elsterian period (OIS 15) and a second during the Upper Elsterian period (OIS 12-11). For the so called Upper interlayer (or "Oberer Zwischenhorizont" - a layer of organic-rich and finer-grained deposits), the IR-RF results point to a deposition age of around 300 ka, with samples taken directly on top and out of this layer yielding IR-RF ages of 288 ± 19 ka and 302 ± 19 ka, respectively. Hence, the measured IR-RF ages clearly point to a deposition during the Lower Saalian period (OIS 9-8) whereas earlier studies assumed a Cromerian age for the sediments of the Upper Interlayer based on pollen records and also mollusc fauna. The new IR-RF dataset indicates that significant hiatuses are present within the fluvial sediment successions. In particular the Eemian and Upper Saalian deposits are missing in this part of the northern Upper Rhine Graben, as the 300 ka deposits are directly overlain by Weichselian fluvial sediments. It is obvious that time periods of increased fluvial aggradation were interrupted by time periods of almost no aggradation or erosion which should have been mainly triggered by phases of increased and decreased subsidence of the Heidelberg Basin. © 2011 Silesian University of Technology.
- ItemOptical dating of alluvial deposits at the orogenic front of the andean precordillera (Mendoza, Argentina)(Warsaw : De Gruyter, 2012) Schmidt, Silke; Tsukamoto, Sumiko; Salomon, Eric; Frechen, Manfred; Hetzel, RalfWell constrained numerical ages of alluvial fan sediments are key to understanding the chronology of alluvial episodes and tectonic activity at the front of the Andean Precordillera. We test-ed the application of radiocarbon and optically stimulated luminescence (OSL) dating in the distal part of an alluvial fan five kilometers north of Mendoza. For OSL dating a large number of aliquots (n > 70)-each composed of ̃50 quartz grains-were measured in order to obtain reliable burial ages despite scattered dose distributions. Owing to a feldspar contamination in all samples, an infrared stimulation was inserted before each OSL measurement, which reduced the feldspar OSL signal suc-cessfully. By using the minimum age model we obtained stratigraphically consistent burial ages of al-luvial deposits in a depth profile. The uppermost ̃1 m of sediment is composed of debris flow depos-its buried 770±76 years ago. Three plant remnants used for radiocarbon dating from the same layer, however, yielded ages younger than 350 years, which are interpreted to underestimate the deposition-al age. Underneath the debris flow, a major unconformity cuts a series of distal alluvial fan sediments with interstratified floodplain deposits, which are composed of sandy and calcite-rich silt layers, re-spectively. Three samples from this unit which were distributed over one meter of sediment thickness yielded statistically concordant OSL ages of 12.3±1.2 ka, 12.3±1.2 ka, and 11.7±1.1 ka. The deposi-tion of these sediments during the latest Pleistocene coincides with a phase of cool and humid cli-mate, which occurred before the alluvial fan propagated farther into the foreland. The overlying de-bris flow sediments are associated with alluvial fan incision during the arid Late Holocene. © 2011 Silesian University of Technology.