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- ItemClassification and quantification of pore shapes in sandstone reservoir rocks with 3-D X-ray micro-computed tomography(Göttingen : Copernicus Publ., 2016) Schmitt, Mayka; Halisch, Matthias; Müller, Cornelia; Fernandes, Celso PeresRecent years have seen a growing interest in the characterization of the pore morphologies of reservoir rocks and how the spatial organization of pore traits affects the macro behavior of rock–fluid systems. With the availability of 3-D high-resolution imaging, such as x-ray micro-computed tomography (µ-CT), the detailed quantification of particle shapes has been facilitated by progress in computer science. Here, we show how the shapes of irregular rock particles (pores) can be classified and quantified based on binary 3-D images. The methodology requires the measurement of basic 3-D particle descriptors (length, width, and thickness) and a shape classification that involves the similarity of artificial objects, which is based on main pore network detachments and 3-D sample sizes. Two main pore components were identified from the analyzed volumes: pore networks and residual pore ganglia. A watershed algorithm was applied to preserve the pore morphology after separating the main pore networks, which is essential for the pore shape characterization. The results were validated for three sandstones (S1, S2, and S3) from distinct reservoirs, and most of the pore shapes were found to be plate- and cube-like, ranging from 39.49 to 50.94 % and from 58.80 to 45.18 % when the Feret caliper descriptor was investigated in a 10003 voxel volume. Furthermore, this study generalizes a practical way to correlate specific particle shapes, such as rods, blades, cuboids, plates, and cubes to characterize asymmetric particles of any material type with 3-D image analysis.
- ItemPore-scale tomography and imaging: applications, techniques and recommended practice(Göttingen : Copernicus Publ., 2016) Halisch, Matthias; Steeb, Holger; Henkel, Steven; Krawczyk, Charlotte M.[No abstract available]
- ItemEnhanced pore space analysis by use of μ-CT, MIP, NMR, and SIP(Göttingen : Copernicus Publ., 2018) Zhang, Zeyu; Kruschwitz, Sabine; Weller, Andreas; Halisch, MatthiasWe investigate the pore space of rock samples with respect to different petrophysical parameters using various methods, which provide data on pore size distributions, including micro computed tomography (μ-CT), mercury intrusion porosimetry (MIP), nuclear magnetic resonance (NMR), and spectral-induced polarization (SIP). The resulting cumulative distributions of pore volume as a function of pore size are compared. Considering that the methods differ with regard to their limits of resolution, a multiple-length-scale characterization of the pore space is proposed, that is based on a combination of the results from all of these methods. The approach is demonstrated using samples of Bentheimer and Röttbacher sandstone. Additionally, we compare the potential of SIP to provide a pore size distribution with other commonly used methods (MIP, NMR). The limits of resolution of SIP depend on the usable frequency range (between 0.002 and 100 Hz). The methods with similar resolution show a similar behavior of the cumulative pore volume distribution in the overlapping pore size range. We assume that μ-CT and NMR provide the pore body size while MIP and SIP characterize the pore throat size. Our study shows that a good agreement between the pore radius distributions can only be achieved if the curves are adjusted considering the resolution and pore volume in the relevant range of pore radii. The MIP curve with the widest range in resolution should be used as reference.
- ItemX-ray computed tomography investigation of structures in Opalinus Clay fromlarge-scale to small-scale after mechanical testing(Göttingen : Copernicus Publ., 2016) Kaufhold, Annette; Halisch, Matthias; Zacher, Gerhard; Kaufhold, StephanIn the past years X-ray computed tomography (CT) has became more and more common for geoscientific applications and is used from the µm-scale (e.g. for investigations of microfossils or pore-scale structures) up to the dm-scale (full drill cores or soil columns). In this paper we present results from CT imaging and mineralogical investigations of an Opalinus Clay core on different scales and different regions of interest, emphasizing especially the 3-D evaluation and distribution of cracks and their impact on mechanical testing of such material. Enhanced knowledge of the testing behaviour of the Opalinus Clay is of great interest, especially since this material is considered for a long-term radioactive waste disposal and storage facility in Switzerland. Hence, results are compared regarding the mineral (i.e. phase) contrast resolution, the spatial resolution, and the overall scanning speed. With this extensive interdisciplinary scale-down approach it has been possible to characterize the general fracture propagation in comparison to mineralogical and textural features of the Opalinus Clay. Additionally, and as far as we know, a so-called mylonitic zone, located at an intersect of two main fractures, has been observed for the first time for an experimentally deformed Opalinus sample. The multi-scale results are in good accordance to data from naturally deformed Opalinus Clay samples, which enables us to perform systematical research under controlled laboratory conditions. Accompanying 3-D imaging greatly enhances the capability of data interpretation and assessment of such a material.
- ItemLarge-scale electrical resistivity tomography in the Cheb Basin (Eger Rift) at an International Continental Drilling Program (ICDP) monitoring site to image fluid-related structures(Göttingen : Copernicus Publ., 2019) Nickschick, Tobias; Flechsig, Christina; Mrlina, Jan; Oppermann, Frank; Löbig, Felix; Günther, ThomasThe Cheb Basin, a region of ongoing swarm earthquake activity in the western Czech Republic, is characterized by intense carbon dioxide degassing along two known fault zones – the N–S-striking Počatky–Plesná fault zone (PPZ) and the NW–SE-striking Mariánské Lázně fault zone (MLF). The fluid pathways for the ascending CO2 of mantle origin are one of the subjects of the International Continental Scientific Drilling Program (ICDP) project “Drilling the Eger Rift” in which several geophysical surveys are currently being carried out in this area to image the topmost hundreds of meters to assess the structural situation, as existing boreholes are not sufficiently deep to characterize it. As electrical resistivity is a sensitive parameter to the presence of conductive rock fractions as liquid fluids, clay minerals, and also metallic components, a large-scale dipole–dipole experiment using a special type of electric resistivity tomography (ERT) was carried out in June 2017 in order to image fluid-relevant structures. We used permanently placed data loggers for voltage measurements in conjunction with moving high-power current sources to generate sufficiently strong signals that could be detected all along the 6.5 km long profile with 100 and 150 m dipole spacings. After extensive processing of time series for voltage and current using a selective stacking approach, the pseudo-section is inverted, which results in a resistivity model that allows for reliable interpretations depths of up than 1000 m. The subsurface resistivity image reveals the deposition and transition of the overlying Neogene Vildštejn and Cypris formations, but it also shows a very conductive basement of phyllites and granites that can be attributed to high salinity or rock alteration by these fluids in the tectonically stressed basement. Distinct, narrow pathways for CO2 ascent are not observed with this kind of setup, which hints at wide degassing structures over several kilometers within the crust instead. We also observed gravity and GPS data along this profile in order to constrain ERT results. A gravity anomaly of ca. −9 mGal marks the deepest part of the Cheb Basin where the ERT profile indicates a large accumulation of conductive rocks, indicating a very deep weathering or alteration of the phyllitic basement due to the ascent of magmatic fluids such as CO2. We propose a conceptual model in which certain lithologic layers act as caps for the ascending fluids based on stratigraphic records and our results from this experiment, providing a basis for future drillings in the area aimed at studying and monitoring fluids.