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Now showing 1 - 10 of 13
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    Funnel-shaped microstructures for strong reversible adhesion
    (Hoboken, NJ : Wiley, 2017) Fischer, Sarah C.L.; GroĂŸ, Katja; Abad, Oscar Torrents; Becker, MIchael M.; Park, Euiyoung; Hensel, RenĂ©; Arzt, Eduard
    The potential of a new design of adhesive microstructures in the micrometer range for enhanced dry adhesion is investigated. Using a two-photon lithography system, complex 3D master structures of funnel-shaped microstructures are fabricated for replication into poly(ethylene glycol) dimethacrylate polymer. The diameter, the flap thickness, and the opening angle of the structures are varied systematically. The adhesion of single structures is characterized using a triboindenter system equipped with a flat diamond punch. The pull-off stresses obtained reaches values up to 5.6 MPa, which is higher than any values reported in literature for artificial dry adhesives. Experimental and numerical results suggest a characteristic attachment mechanism that leads to intimate contact formation from the edges toward the center of the structures. van der Waals interactions most likely dominate the adhesion, while contributions by suction or capillarity play only a minor role. Funnel-shaped microstructures are a promising concept for strong and reversible adhesives, applicable in novel pick and place handling systems or wall-walking robots.
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    Engineering Micropatterned Dry Adhesives: From Contact Theory to Handling Applications
    (Weinheim : Wiley-VCH, 2018) Hensel, René; Moh, Karsten; Arzt, Eduard
    Reversible adhesion is the key functionality to grip, place, and release objects nondestructively. Inspired by nature, micropatterned dry adhesives are promising candidates for this purpose and have attracted the attention of research groups worldwide. Their enhanced adhesion compared to nonpatterned surfaces is frequently demonstrated. An important conclusion is that the contact mechanics involved is at least as important as the surface energy and chemistry. In this paper, the roles of the contact geometry and mechanical properties are reviewed. With a focus on applications, the effects of substrate roughness and of temperature variations, and the long-term performance of micropatterned adhesives are discussed. The paper provides a link between the current, detailed understanding of micropatterned adhesives and emerging applications.
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    Composite pillars with a tunable interface for adhesion to rough substrates
    (Washington D.C. : American Chemical Society, 2017) Fischer, Sarah C.L.; Arzt, Eduard; Hensel, René
    The benefits of synthetic fibrillar dry adhesives for temporary and reversible attachment to hard objects with smooth surfaces have been successfully demonstrated in previous studies. However, surface roughness induces a dramatic reduction in pull-off stresses and necessarily requires revised design concepts. Toward this aim, we introduce cylindrical two-phase single pillars, which are composed of a mechanically stiff stalk and a soft tip layer. Adhesion to smooth and rough substrates is shown to exceed that of conventional pillar structures. The adhesion characteristics can be tuned by varying the thickness of the soft tip layer, the ratio of the Young’s moduli and the curvature of the interface between the two phases. For rough substrates, adhesion values similar to those obtained on smooth substrates were achieved. Our concept of composite pillars overcomes current practical limitations caused by surface roughness and opens up fields of application where roughness is omnipresent.
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    Adhesion and relaxation of a soft elastomer on surfaces with skin like roughness
    (Amsterdam : Elsevier, 2018) Fischer, Sarah; Boyadzhieva, Silviya; Hensel, René; Kruttwig, Klaus; Arzt, Eduard
    For designing new skin adhesives, the complex mechanical interaction of soft elastomers with surfaces of various roughnesses needs to be better understood. We systematically studied the effects of a wide set of roughnesscharacteristics, film thickness, hold time and material relaxation on the adhesive behaviour of the silicone elastomer SSA 7–9800 (Dow Corning). As model surfaces, we used epoxy replicas obtained from substrates with roughness ranging from very smooth to skin-like. Our results demonstrate that films of thin and intermediate thickness (60 and 160 μm) adhered best to a sub-micron rough surface, with a pull-off stress of about 50 kPa. Significant variations in pull-off stress and detachment mechanism with roughness and hold time were found. In contrast, 320 μm thick films adhered with lower pull-off stress of about 17 kPa, but were less sensitive to roughness and hold time. It is demonstrated that the adhesion performance of the siliconefilms to rough surfaces can be tuned by tailoring the film thickness and contact time.
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    Cohesive detachment of an elastic pillar from a dissimilar substrate
    (Amsterdam : Elsevier, 2017) Fleck, Norman A.; Khaderi, Syed Nizamuddin; McMeeking, Robert M.; Arzt, Eduard
    The adhesion of micron-scale surfaces due to intermolecular interactions is a subject of in- tense interest spanning electronics, biomechanics and the application of soft materials to engineering devices. The degree of adhesion is sensitive to the diameter of micro-pillars in addition to the degree of elastic mismatch between pillar and substrate. Adhesion- strength-controlled detachment of an elastic circular cylinder from a dissimilar substrate is predicted using a Dugdale-type of analysis, with a cohesive zone of uniform tensile strength emanating from the interface corner. Detachment initiates when the opening of the cohesive zone attains a critical value, giving way to crack formation. When the cohe- sive zone size at crack initiation is small compared to the pillar diameter, the initiation of detachment can be expressed in terms of a critical value H c of the corner stress inten- sity. The estimated pull-offforce is somewhat sensitive to the choice of stick/slip boundary condition used on the cohesive zone, especially when the substrate material is much stiffer than the pillar material. The analysis can be used to predict the sensitivity of detachment force to the size of pillar and to the degree of elastic mismatch between pillar and sub- strate.
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    Numerical study of adhesion enhancement by composite fibrils with soft tip layers
    (Amsterdam : Elsevier, 2016) Balijepalli, Ram Gopal; Fischer, Sarah C.L.; Hensel, René; McMeeking, Robert M.; Arzt, Eduard
    Bio-inspired fibrillar surfaces with reversible adhesion to stiff substrates have been thoroughly investigated over the last decade. In this paper we propose a novel composite fibril consisting of a soft tip layer and stiffer stalk with differently shaped interfaces (flat vs. curved) between them. A tensile stress is applied remotely on the free end of the fibril whose other end adheres to a rigid substrate. The stress distributions and the resulting adhesion of such structures were numerically investigated under plane strain (2D) and axisymmetric (3D) conditions. The stress intensities were evaluated for different combinations of layer thickness and Young’s moduli. The adhesion strength values were found to increase for thinner layers and larger modulus ratio; these trends are also reflected in selected experimental results. The results of this paper provide a new strategy for optimizing adhesion strength of fibrillar surfaces.
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    Elevated temperature adhesion of bioinspired polymeric micropatterns to glass
    (Amsterdam : Elsevier, 2017) Barreau, Viktoriia; Yu, Dan; Hensel, René; Arzt, Eduard
    Micropatterned polymer surfaces that operate at various temperatures are required for emerging technical applications such as handling of objects or space debris. As the mechanical properties of polymers can vary significantly with temperature, adhesion performance can exhibit large variability. In the present paper, we experimentally study temperature effects on the adhesion of micropatterned adhesives (pillar length 20 μm, aspect ratios 0.4 and 2) made from three different polymers, i.e., polydimethylsiloxane (PDMS), perfluoropolyether dimethacrylate (PFPEdma), and polyurethane (PU-ht). PU specimens showed the highest pull-off stresses of about 57 kPa at 60 °C, i.e., more than twice the value of unpatterned control samples. The work of separation similarly showed a maximum at that temperature, which was identified as the glass transition temperature, Tg. PDMS and PFPEdma specimens were tested above their Tg. As a result, the adhesion properties decreased monotonically (about 50% for both materials) for temperature elevation from 20 to 120 °C. Overall, the results obtained in our study indicate that the operating temperature related to the glass transition temperature should be considered as a significant parameter for assessing the adhesion performance of micropatterned adhesives and in the technical design of adhesion devices.
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    The role of the backing layer in the mechanical properties of micrometer-scale fibrillar structures
    (SaarbrĂ¼cken : Leibniz-Institut fĂ¼r Neue Materialien, 2010) Guidoni, Griselda; Schillo, Dominik; Hangen, Ude; Castellanos, Graciela; Arzt, Eduard; McMeeking, Robert; Bennewitz, Roland
    The contact mechanics of a micro-fabricated fibrillar surface structure made of poly(dimethylsiloxane) (PDMS) was studied in this work. The attachment and detachment of individual fibrils to and from a spherical indenter upon approach and retraction are detected as jumps in force and stiffness. A quantitative model describes the jumps in stiffness values by taking into account the deformation of the backing layer. The results emphasize the importance of long-range interactions in the contact mechanics of elastic materials and confirm the concepts underlying the development of fibrillar adhesive materials.
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    Size dependent strength of bcc metal micropillars: towards high strength surfaces by micropatterning
    (SaarbrĂ¼cken : Leibniz-Institut fĂ¼r Neue Materialien, 2010) Schneider, Andreas; Arzt, Eduard
    The size effect in body-centered cubic (bcc) metals was comprehensively investigated through microcompression tests performed on focused ion beam machined tungsten (W), molybdenum (Mo) and niobium (Nb) pillars, with single slip [235] and multiple slip [001] orientations. The relationship between yield strength and pillar diameter as well as the deformation morphologies were found to correlate with a parameter specific for bcc metals, i.e. the critical temperature Tc. This finding sheds new light on the phenomenon of small-scale plasticity in largely unexplored non-fcc metals. This effect may be used in the patterning of surfaces to achieve higher strengths.
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    A Design Strategy for Mushroom-Shaped Microfibrils With Optimized Dry Adhesion: Experiments and Finite Element Analyses
    (New York, NY : ASME, 2021) Zhang, Xuan; Wang, Yue; Hensel, René; Arzt, Eduard
    Enhanced dry adhesion of micropatterned polymeric surfaces has been frequently demonstrated. Among the design parameters, the cap geometry plays an important role to improve their performance. In this study, we combined experiments on single polyurethane mushroom-shaped fibrils (with a stalk diameter of 80 µm and height of 125 µm) against flat glass, with numerical simulations implementing a cohesive zone. We found that the geometry of the mushroom cap strongly affects the interfacial crack behavior and the pull-off stress. The experimental and numerical results suggest that optimal adhesion was accompanied by the appearance of both edge and interior interfacial cracks during separation. Finite elemental analyses revealed the evolution of the interfacial stress distributions as a function of the cap thickness and confirmed the distinct detachment mechanisms. Furthermore, the effect of the stalk diameter and the Young's modulus on the adhesive force was established, resulting in an optimal design for mushroom-shaped fibrils.