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Geophysical investigation of a freshwater lens on the island of Langeoog, Germany – Insights from combined HEM, TEM and MRS data

2017, Costabel, Stephan, Siemon, Bernhard, Houben, Georg, Günther, Thomas

A multi-method geophysical survey, including helicopter-borne electromagnetics (HEM), transient electromagnetics (TEM), and magnetic resonance sounding (MRS), was conducted to investigate a freshwater lens on the North Sea island of Langeoog, Germany. The HEM survey covers the entire island and gives an overview of the extent of three freshwater lenses that reach depths of up to 45 m. Ground-based TEM and MRS were conducted particularly on the managed western lens to verify the HEM results and to complement the lithological information from existing boreholes. The results of HEM and TEM are in good agreement. Salt- and freshwater-bearing sediments can, as expected, clearly be distinguished due to their individual resistivity ranges. In the resistivity data, a large transition zone between fresh- and saltwater with a thickness of up to 20 m is identified, the existence of which is verified by borehole logging and sampling. Regarding lithological characterisation of the subsurface, the MRS method provides more accurate and reliable results than HEM and TEM. Using a lithological index derived from MRS water content and relaxation time, thin aquitard structures as well as fine and coarse sand aquifers can be distinguished. Complementing the existing borehole data with the lithology information estimated from MRS, we generate a map showing the occurrence of aquitard structures, which significantly improves the hydrogeological model of the island. Moreover, we demonstrate that the estimates of groundwater conductivity in the sand aquifers from geophysical data are in agreement with the fluid conductivity measured in the boreholes.

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Hydraulic characterisation of iron-oxide-coated sand and gravel based on nuclear magnetic resonance relaxation mode analyses

2018, Costabel, Stephan, Weidner, Christoph, Müller-Petke, Mike, Houben, Georg

The capability of nuclear magnetic resonance (NMR) relaxometry to characterise hydraulic properties of iron-oxide-coated sand and gravel was evaluated in a laboratory study. Past studies have shown that the presence of paramagnetic iron oxides and large pores in coarse sand and gravel disturbs the otherwise linear relationship between relaxation time and pore size. Consequently, the commonly applied empirical approaches fail when deriving hydraulic quantities from NMR parameters. Recent research demonstrates that higher relaxation modes must be taken into account to relate the size of a large pore to its NMR relaxation behaviour in the presence of significant paramagnetic impurities at its pore wall. We performed NMR relaxation experiments with water-saturated natural and reworked sands and gravels, coated with natural and synthetic ferric oxides (goethite, ferrihydrite), and show that the impact of the higher relaxation modes increases significantly with increasing iron content. Since the investigated materials exhibit narrow pore size distributions, and can thus be described by a virtual bundle of capillaries with identical apparent pore radius, recently presented inversion approaches allow for estimation of a unique solution yielding the apparent capillary radius from the NMR data. We found the NMR-based apparent radii to correspond well to the effective hydraulic radii estimated from the grain size distributions of the samples for the entire range of observed iron contents. Consequently, they can be used to estimate the hydraulic conductivity using the well-known Kozeny–Carman equation without any calibration that is otherwise necessary when predicting hydraulic conductivities from NMR data. Our future research will focus on the development of relaxation time models that consider pore size distributions. Furthermore, we plan to establish a measurement system based on borehole NMR for localising iron clogging and controlling its remediation in the gravel pack of groundwater wells.

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Noninvasive Estimation of Water Retention Parameters by Observing the Capillary Fringe with Magnetic Resonance Sounding

2014, Costabel, Stephan, Günther, Thomas

The magnetic resonance sounding (MRS) method is usually applied for delineation and characterization of aquifer system stratification. Its unique property, distinct from other hydrogeophysical methods, is the direct sensitivity to water content in the subsurface. The inversion of MRS data yields the subsurface water content distribution without need of a petrophysical model. Recent developments in instrumentation, i.e., decreased instrumental dead times and advanced noise cancellation strategies, enable the use of this method for investigating the vadose zone. A possible way to interpret MRS measurements with focus on water retention (WR) parameters is an inversion approach that directly provides WR parameters by modeling the capillary fringe (CF inversion). We have developed this kind of inversion further to account for different WR models and present a sensitivity study based on both synthetic and real field data. To assess the general applicability of the CF inversion, we analyzed the resolution properties for different measurement layouts and the parameter uncertainties for different realistic scenarios. Under moderate noise conditions and if the water table position is known, all WR parameters except the residual water content can be reliably estimated. The relative accuracy of the estimated pore distribution index estimation is better for larger CF. Small measurement loops of 5-m diameter achieve the best resolution for shallow investigation depths of <10 m.

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Comparison of novel semi-airborne electromagnetic data with multi-scale geophysical, petrophysical and geological data from Schleiz, Germany

2020, Steuer, Annika, Smirnova, Maria, Becken, Michael, Schiffler, Markus, Günther, Thomas, Rochlitz, Raphael, Yogeshwar, Pritam, Mörbe, Wiebke, Siemon, Bernhard, Costabel, Stephan, Preugschat, Benedikt, Ibs-von Seht, Malte, Zampa, Luigi Sante, Müller, Franz

In the framework of the Deep Electromagnetic Sounding for Mineral EXploration (DESMEX) project, we carried out multiple geophysical surveys from regional to local scales in a former mining area in the state of Thuringia, Germany. We prove the applicability of newly developed semi-airborne electromagnetic (EM) systems for mineral exploration by cross-validating inversion results with those of established airborne and ground-based investigation techniques. In addition, supporting petrophysical and geological information to our geophysical measurements allowed the synthesis of all datasets over multiple scales. An initial regional-scale reconnaissance survey was performed with BGR's standard helicopter-borne geophysical system deployed with frequency-domain electromagnetic (HEM), magnetic and radiometric sensors. In addition to geological considerations, the HEM results served as base-line information for the selection of an optimal location for the intermediate-scale semi-airborne EM experiments. The semi-airborne surveys utilized long grounded transmitters and two independent airborne receiver instruments: induction coil magnetometers and SQUID sensors. Due to the limited investigation depth of the HEM method, local-scale electrical resistivity tomography (ERT) and long-offset transient electromagnetic (LOTEM) measurements were carried out on a reference profile, enabling the validation of inversion results at greater depths. The comparison of all inversion results provided a consistent overall resistivity distribution. It further confirmed that both semi-airborne receiver instruments achieve the bandwidth and sensitivity required for the investigation of the resistivity structure down to 1 km depth and therewith the detection of deeply seated earth resources. A 3D geological model, lithological and geophysical borehole logs as well as petrophysical investigations were integrated to interpret of the geophysical results. Distinct highly-conductive anomalies with resistivities of less than 10 Om were identified as alum shales over all scales. Apart from that, the petrophysical investigations exhibited that correlating geophysical and geological information using only one single parameter, such as the electrical resistivity, is hardly possible. Therefore, we developed a first approach based on clustering methods and self-organizing maps (SOMs) that allowed us to assign geological units at the surface to a given combination of geophysical and petrophysical parameters, obtained on different scales. © 2020 The Authors

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Soil hydraulic interpretation of nuclear magnetic resonance measurements based on circular and triangular capillary models

2021, Costabel, Stephan, Hiller, Thomas

Geophysical nuclear magnetic resonance (NMR) applications are used to estimate pore size distributions (PSDs) of rocks and sediments. This is commonly realized by empirical calibration using information about the surface-to-volume ratio of the material. Recent research has developed joint inversion concepts for NMR relaxation data that provides the PSD with a minimum of information. The application requires the NMR signal of a sample at saturation and at least one at partial saturation and at known suction. The new inversion concept physically simulates the desaturation process as part of the forward operator. The cross-section of the model capillaries in the underlying bundle can be either circular or triangular. Our study investigates the performance of the NMR joint inversion to predict water retention function (WRF) and capillary-based hydraulic conductivity (Kcap) as functions of saturation for different sands. The angularity of the pores has no significant impact on the estimated WRF but affects the Kcap estimation significantly. Our study shows that the WRF is predicted reliably for sand samples under fast diffusion conditions. The Kcap estimations are also plausible but tend to systematic overestimation, for which we identified the tortuosity being the main reason. Because NMR relaxation data generally do not provide tortuosity information, a plausible tortuosity model remains an issue of classical calibration. Further development of the approach will thus consider tortuosity measurements (e.g., by electrical resistivity measurements and/or gradient NMR) and will consider the relaxation mechanisms outside fast diffusion conditions to enhance its applicability for coarse soils.

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Evaluation of single-sided nuclear magnetic resonance technology for usage in geosciences

2022, Costabel, Stephan, Hiller, Thomas, Dlugosch, Raphael, Kruschwitz, Sabine, Müller-Petke, Mike

Because of its mobility and ability to investigate exposed surfaces, single-sided (SiS) nuclear magnetic resonance (NMR) technology enables new application fields in geosciences. To test and assess its corresponding potential, we compare longitudinal (T 1) and transverse (T 2) data measured by SiS NMR with those of conventional geoscientific laboratory NMR. We use reference sandstone samples covering a broad range of pore sizes. Our study demonstrates that the lower signal-to-noise ratio of SiS NMR data generally tends to slightly overestimated widths of relaxation time distributions and consequently pore size distributions. While SiS and conventional NMR produce very similar T 1 relaxation data, unbiased SiS NMR results for T 2 measurements can only be expected for fine material, i.e. clayey or silty sediments and soils with main relaxation times below 0.05s . This limit is given by the diffusion relaxation rate due to the gradient in the primary magnetic field associated with the SiS NMR. Above that limit, i.e. for coarse material, the relaxation data is strongly attenuated. If considering the diffusion relaxation time of 0.2 s in the numerical data inversion process, the information content >0.2s is blurred over a range larger than that of conventional NMR. However, our results show that principle range and magnitudes of the relaxation time distributions are reconstructed to some extent. Regarding these findings, SiS NMR can be helpful to solve geoscientific issues, e.g. to assess the hydro-mechanical properties of the walls of underground facilities or to provide local soil moisture data sets for calibrating indirect remote techniques on the regional scale. The greatest opportunity provided by the SiS NMR technology is the acquisition of profile relaxation data for rocks with significant bedding structures at the μm scale. With this unique feature, SiS NMR can support the understanding and modeling of hydraulic and diffusional anisotropy behavior of sedimentary rocks.

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Feasibility study on prepolarized surface nuclear magnetic resonance for soil moisture measurements

2021, Hiller, Thomas, Costabel, Stephan, Radić, Tino, Dlugosch, Raphael, Müller‐Petke, Mike

In the past few years, small-scale (2 m) prepolarized surface nuclear magnetic resonance (SNMR) has gained increasing interest in the research community. As recent studies demonstrated, the application of a strong prepolarization field enhances the SNMR signal of coils with a footprint <1 m2 up to a level that even enables investigations in urban areas. In particular, it is expected that this noninvasive method provides the soil moisture distribution in the upper 2 m of the subsurface in the near future. However, until now all field experiments have been carried out on water reservoirs only, in an approach to test and implement this rather new technique into the field of SNMR applications. We present the first prepolarized SNMR measurement on a real soil and demonstrate the general feasibility of this technique to qualitatively and quantitatively detect soil moisture in the upper first 0.5 m. Our soil moisture measurements are validated by independent time domain reflectometry data. To complement the field experiments with numerical simulations, we adapted the underlying SNMR spin dynamics simulations and account for prepolarization switch-off effects in the forward modeling of the SNMR excitation.