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Now showing 1 - 4 of 4
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    On the fundamental relation of laser schlieren deflectometry for temperature measurements in filamentary plasmas
    (Les Ulis : EDP Sciences, 2015) Schäfer, Jan; Bonaventura, Zdeněk; Foest, Rüdiger
    Recently, laser schlieren deflectometry (LSD) had been successfully employed as a temperature measurement method to reveal the heat convection generated by micro filaments of a self-organized non-thermal atmospheric plasma jet. Based on the theory of the temperature measurements using LSD, in this work, three approaches for an application of the method are introduced: (i) a hyperbolic-like model of refractive index is applied which allows an analytical theory for the evaluation of the deflection angle to be developed, (ii) a Gaussian shape model for the filament temperature is implemented which is analyzed numerically and (iii) an experimental calibration of the laser deflection with a gas mixture of helium and argon is performed. Thus, these approaches demonstrate that a universal relation between the relative maximum temperature of the filament core (T1/T0) and a the maximum deflection angle δ1 of the laser beam can be written as T1/T0=(1 − δ1/δ0)−1, where δ0 is a parameter that is defined by the configuration of the experiment and by the assumed model for the shape of the temperature profile.
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    Plasma-based VAD process for multiply doped glass powders and high-performance fiber preforms with outstanding homogeneity
    (Hoboken, NJ : Wiley Interscience, 2020) Trautvetter, Tom; Schäfer, Jan; Benzine, Omar; Methling, Ralf; Baierl, Hardy; Reichel, Volker; Dellith, Jan; Köpp, Daniel; Hempel, Frank; Stankov, Marjan; Baeva, Margarita; Foest, Rüdiger; Wondraczek, Lothar; Wondraczek, Katrin; Bartelt, Hartmut
    An innovative approach using the vapor axial deposition (VAD), for the preparation of silica-based high-power fiber laser preforms, is described in this study. The VAD uses a plasma deposition system operating at atmospheric pressure, fed by a single, chemically adapted solution containing precursors of laser-active dopants (e.g., Yb2O3), glass-modifier species (e.g., Al2O3), and the silica matrix. The approach enables simultaneous doping with multiple optically active species and overcomes some of the current technological limitations encountered with well-established fiber preform technologies in terms of dopant distribution, doping levels, and achievable active core diameter. The deposition of co-doped silica with outstanding homogeneity is proven by Raman spectroscopy and electron probe microanalysis. Yb2O3 concentrations are realized up to 0.3 mol% in SiO2, with simultaneous doping of 3 mol% of Al2O3.
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    Searching for order in atmospheric pressure plasma jets
    (Bristol : IOP Publ., 2017-11-10) Schäfer, Jan; Sigeneger, Florian; Šperka, Jiří; Rodenburg, Cornelia; Foest, Rüdiger
    The self-organized discharge behaviour occurring in a non-thermal radio-frequency plasma jet in rare gases at atmospheric pressure was investigated. The frequency of the azimuthal rotation of filaments in the active plasma volume and their inclination were measured along with the gas temperature under varying discharge conditions. The gas flow and heating were described theoretically by a three-dimensional hydrodynamic model. The rotation frequencies obtained by both methods qualitatively agree. The results demonstrate that the plasma filaments forming an inclination angle α with the axial gas velocity uz are forced to a transversal movement with the velocity uφ=tan(α)*uz, which is oriented in the inclination direction. Variations of ${u}_{\phi }$ in the model reveal that the observed dynamics minimizes the energy loss due to convective heat transfer by the gas flow. The control of the self-organization regime motivates the application of the plasma jet for precise and reproducible material processing.
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    Liquid assisted plasma enhanced chemical vapour deposition with a non-thermal plasma jet at atmospheric pressure
    (Amsterdam [u.a.] : Elsevier, 2016) Schäfer, Jan; Fricke, Katja; Mika, Filip; Pokorná, Zuzana; Zajíčková, Lenka; Foest, Rüdiger
    The present study introduces a process for the synthesis of functional films onto substrates directly from the liquid phase. The reported method is based on the initialization of the synthesis by means of an atmospheric pressure plasma jet operating with argon above a thin liquid film of the starting material. The process is demonstrated by the formation of a thin, solid SiOx film from siloxane-based liquid precursors. Changes in the chemical properties of the precursor were studied in-situ during the polymerization process on the diamond crystal by using Fourier transform infrared spectroscopy The elemental composition of the SiOxCy films was analyzed by X-ray photoelectron spectroscopy (XPS). Furthermore, XPS was applied to study the effect of post-annealing processes on the composition of the films. The obtained deposits exhibit a low concentration of carbon groups. The amount of hydroxyl groups and interstitial water can be reduced significantly by post-process annealing of the films.