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- ItemCarboxylated nitrile butadiene rubber/hybrid filler composites(São Carlos : Universidade Federal de São Carlos, 2012) Mousa, A.; Heinrich, G.; Simon, F.; Wagenknecht, U.; Stöckelhuber, K.-W.; Dweiri, R.The surface properties of the OSW and NLS are measured with the dynamic contact-angle technique. The x-ray photoelectron spectroscopy (XPS) of the OSW reveals that the OSW possesses various reactive functional groups namely hydroxyl groups (OH). Hybrid filler from NLS and OSW were incorporated into carboxylated nitrile rubber (XNBR) to produce XNBR hybrid composites. The reaction of OH groups from the OSW with COOH of the XNBR is checked by attenuated total reflectance spectra (ATR-IR) of the composites. The degree of curing ΔM (maximum torque-minimum torque) as a function of hybrid filler as derived from moving die rheometer (MDR) is reported. The stress-strain behavior of the hybrid composites as well as the dynamic mechanical thermal analysis (DMTA) is studied. Bonding quality and dispersion of the hybrid filler with and in XNBR are examined using scanning-transmission electron microscopy (STEM in SEM).
- ItemA numerical study on deformation of Newtonian droplets through converging cylindrical dies(Berlin : de Gruyter, 2013) Mostafaiyan, M.; Saeb, M.R.; Ahmadi, Z.; Khonakdar, H.A.; Wagenknecht, U.; Heinrich, G.In this work, the dynamic deformation of a viscose Newtonian droplet passing through cylindrical converging dies has been studied. The changes in the interfacial area between two immiscible Newtonian fluids have been considered as a variable representing the time-dependent deformation of a circular droplet along converging dies. To do so, a surface tracking method has been incorporated into a finite element code, developed by the authors, which quantifies the deformation of the droplet through the converging path, and where the surface area of the deformed drop has been consequently chosen as a criterion for a two-phase interface. In this study, it has been revealed that by changing both rheological and geometrical parameters it is possible to manage the value of interface area between two phases. Ultimately, a unique curve is developed for each droplet to primary phase viscosity ratio which can correlate drop deformation with geometrical parameters.