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Crystal structure of η5-3,6-di-tert-butyl-4- (tris(pentafluorophenyl)boranyloxycarbonyl)-5-(η5- tetramethylcyclopentadienyl-methyl-9,10,11-trimethyl-bicyclo(6.3.0) undeca-4-en-8,10-dienyl)titanium(III) toluene hemisolvate, Ti(C 51H47BF15O2) · 0.5C 7H8
C54.50H51BF15O2Ti, triclinic, P1̄ (no. 2), a = 11.603(2) Å, b = 12.872(3) Å, c = 18.142(4) Å, α = 76.47(3)°, β = 77.99(3)°, γ = 69.13(3)°, V = 2438.2 Å5, Z = 2, Rgt(F) = 0.048, wRobs(F2) = 0.114, T = 200 K. © by Oldenbourg Wissenchaftsverlag.
Crystal structure of η5-1-(tris(pentafluorophenyl) boranylmethyl)-2,3,4,5-tetramethylcyclopentadienyl-η5, η1-3,6-di-tert-butyl-9,10,11-trimethyl-bicyclo(6.3.0) undeca-3-en-8,10-dienyl)titanium(IV),Ti(C50H48BF 15)
C50H48BF15Ti, monoclinic, P12 1/c1 (no. 14), a = 12.007(2) Å, b = 19.511(4) Å, c = 20.010(4) Å, β = 98.90(3)°, V= 4631.3 Å3, Z = 4, Rgt(F) = 0.052, wRref(F2) = 0.120, T = 200 K. © by Oldenbourg Wissenchaftsverlag.
Crystal structures of tribromo(η5-3,6-di-tert-butyl-9,10,11- trimethyl-bicyclo(6.3.0)undeca-4-en-8,10-dienyl)titanium(IV), Ti(C 22H35)Br3, and tribromo(η5-4,5- dibromo-3,6-di-tert-butyl-9,10,11-trimethyl-bicyclo(6.3.0)undeca-8,10-dienyl) titanium(IV), Ti(C22H35Br2)Br3
C22H35Br3Ti, triclinic, P1̄ (no. 2), a = 9.621(2) Å, b = 11.796(2) Å, c = 12.232(2) Å, α = 102.23(3)°, β = 97.71(3)°, γ = 112.32(3)°, V = 1219.2 Å3, Z = 2, Rgt(F) = 0.058, wRobs(F 2) = 0.134, T = 293 K. C22H35Br5Ti, monoclinic, P121/n1 (no. 14), a = 7.474(1) Å, b = 18.458(4) Å, c = 20.171(4) Å, β = 100.28(3)°, V= 2738.0 Å3, Z = 4, Rgt(F) = 0.054, wRobs(F 2) = 0.119, T = 293 K. © by Oldenbourg Wissenchaftsverlag.