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Langer, P.
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Mamat, C.
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Reinke, H.
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[3+3] cyclization
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19F NMR Spectroscopy
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CF3 salicylates
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X-Ray crystallography
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2009
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2020
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Berlin : de Gruyter
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Zeitschrift für Naturforschung - Section B Journal of Chemical Sciences 64 (2009), Nr. 4
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NMR studies and crystal structure determinations of CF3 group-containing bieyelie phenolates
(
Berlin : de Gruyter,
2009
)
Mamat, C.
;
Reinke, H.
;
Langer, P.
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Three new CF3-substituted bicyclic salicylate derivatives were synthesized by the TiCl4-mediated cyclization of trifluoromethyl- containing ketones with l,3-bis(silyl enol ethers) and characterized by NMR and IR, spectroscopy, mass spectrometry and elemental analysis. The crystal structures of the bicyclic derivatives have been determined by single crystal X-ray analysis. All structures exhibit hydrogen bonding. © 2009 Verlag der Zeitschrift für Naturforschung.
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