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End date: 2021 × Start date: 2020 × Subject: Pore size × WGL Institute: LIAG ×

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    Benchmark study using a multi-scale, multi-methodological approach for the petrophysical characterization of reservoir sandstones
    (Göttingen : Copernicus Publ., 2021) Haruzi, Peleg; Katsman, Regina; Halisch, Matthias; Waldmann, Nicolas; Spiro, Baruch
    This paper presents a detailed description and evaluation of a multi-methodological petrophysical approach for the comprehensive multi-scale characterization of reservoir sandstones. The suggested methodology enables the identification of links between Darcy-scale permeability and an extensive set of geometrical, textural and topological rock descriptors quantified at the pore scale. This approach is applied to the study of samples from three consecutive sandstone layers of Lower Cretaceous age in northern Israel. These layers differ in features observed at the outcrop, hand specimen, petrographic microscope and micro-CT scales. Specifically, laboratory porosity and permeability measurements of several centimetre-sized samples show low variability in the quartz arenite (top and bottom) layers but high variability in the quartz wacke (middle) layer. The magnitudes of this variability are also confirmed by representative volume sizes and by anisotropy evaluations conducted on micro-CT-imaged 3-D pore geometries. Two scales of directional porosity variability are revealed in quartz arenite sandstone of the top layer: the pore size scale of ∼0.1 mm in all directions and ∼3.5 mm scale related to the occurrence of high- and low-porosity horizontal bands occluded by Fe oxide cementation. This millimetre-scale variability controls the laboratory-measured macroscopic rock permeability. More heterogeneous pore structures were revealed in the quartz wacke sandstone of the intermediate layer, which shows high inverse correlation between porosity and clay matrix in the vertical direction attributed to depositional processes and comprises an internal spatial irregularity. Quartz arenite sandstone of the bottom layer is homogenous and isotropic in the investigated domain, revealing porosity variability at a ∼0.1 mm scale, which is associated with the average pore size. Good agreement between the permeability upscaled from the pore-scale modelling and the estimates based on laboratory measurements is shown for the quartz arenite layers. The proposed multi-methodological approach leads to an accurate petrophysical characterization of reservoir sandstones with broad ranges of textural, topological and mineralogical characteristics and is particularly applicable for describing anisotropy and heterogeneity of sandstones on various rock scales. The results of this study also contribute to the geological interpretation of the studied stratigraphic units.
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    Soil hydraulic interpretation of nuclear magnetic resonance measurements based on circular and triangular capillary models
    (Hoboken, NJ : Wiley, 2021) Costabel, Stephan; Hiller, Thomas
    Geophysical nuclear magnetic resonance (NMR) applications are used to estimate pore size distributions (PSDs) of rocks and sediments. This is commonly realized by empirical calibration using information about the surface-to-volume ratio of the material. Recent research has developed joint inversion concepts for NMR relaxation data that provides the PSD with a minimum of information. The application requires the NMR signal of a sample at saturation and at least one at partial saturation and at known suction. The new inversion concept physically simulates the desaturation process as part of the forward operator. The cross-section of the model capillaries in the underlying bundle can be either circular or triangular. Our study investigates the performance of the NMR joint inversion to predict water retention function (WRF) and capillary-based hydraulic conductivity (Kcap) as functions of saturation for different sands. The angularity of the pores has no significant impact on the estimated WRF but affects the Kcap estimation significantly. Our study shows that the WRF is predicted reliably for sand samples under fast diffusion conditions. The Kcap estimations are also plausible but tend to systematic overestimation, for which we identified the tortuosity being the main reason. Because NMR relaxation data generally do not provide tortuosity information, a plausible tortuosity model remains an issue of classical calibration. Further development of the approach will thus consider tortuosity measurements (e.g., by electrical resistivity measurements and/or gradient NMR) and will consider the relaxation mechanisms outside fast diffusion conditions to enhance its applicability for coarse soils.