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DDC: 550 × Has files: Yes × Publisher: Göttingen : Copernicus Publ. × Subject: Tomography × Subject: tomography ×

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    Classification and quantification of pore shapes in sandstone reservoir rocks with 3-D X-ray micro-computed tomography
    (Göttingen : Copernicus Publ., 2016) Schmitt, Mayka; Halisch, Matthias; Müller, Cornelia; Fernandes, Celso Peres
    Recent years have seen a growing interest in the characterization of the pore morphologies of reservoir rocks and how the spatial organization of pore traits affects the macro behavior of rock–fluid systems. With the availability of 3-D high-resolution imaging, such as x-ray micro-computed tomography (µ-CT), the detailed quantification of particle shapes has been facilitated by progress in computer science. Here, we show how the shapes of irregular rock particles (pores) can be classified and quantified based on binary 3-D images. The methodology requires the measurement of basic 3-D particle descriptors (length, width, and thickness) and a shape classification that involves the similarity of artificial objects, which is based on main pore network detachments and 3-D sample sizes. Two main pore components were identified from the analyzed volumes: pore networks and residual pore ganglia. A watershed algorithm was applied to preserve the pore morphology after separating the main pore networks, which is essential for the pore shape characterization. The results were validated for three sandstones (S1, S2, and S3) from distinct reservoirs, and most of the pore shapes were found to be plate- and cube-like, ranging from 39.49 to 50.94 % and from 58.80 to 45.18 % when the Feret caliper descriptor was investigated in a 10003 voxel volume. Furthermore, this study generalizes a practical way to correlate specific particle shapes, such as rods, blades, cuboids, plates, and cubes to characterize asymmetric particles of any material type with 3-D image analysis.
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    X-ray computed tomography investigation of structures in Opalinus Clay fromlarge-scale to small-scale after mechanical testing
    (Göttingen : Copernicus Publ., 2016) Kaufhold, Annette; Halisch, Matthias; Zacher, Gerhard; Kaufhold, Stephan
    In the past years X-ray computed tomography (CT) has became more and more common for geoscientific applications and is used from the µm-scale (e.g. for investigations of microfossils or pore-scale structures) up to the dm-scale (full drill cores or soil columns). In this paper we present results from CT imaging and mineralogical investigations of an Opalinus Clay core on different scales and different regions of interest, emphasizing especially the 3-D evaluation and distribution of cracks and their impact on mechanical testing of such material. Enhanced knowledge of the testing behaviour of the Opalinus Clay is of great interest, especially since this material is considered for a long-term radioactive waste disposal and storage facility in Switzerland. Hence, results are compared regarding the mineral (i.e. phase) contrast resolution, the spatial resolution, and the overall scanning speed. With this extensive interdisciplinary scale-down approach it has been possible to characterize the general fracture propagation in comparison to mineralogical and textural features of the Opalinus Clay. Additionally, and as far as we know, a so-called mylonitic zone, located at an intersect of two main fractures, has been observed for the first time for an experimentally deformed Opalinus sample. The multi-scale results are in good accordance to data from naturally deformed Opalinus Clay samples, which enables us to perform systematical research under controlled laboratory conditions. Accompanying 3-D imaging greatly enhances the capability of data interpretation and assessment of such a material.