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Inter-granular effects at high magnetic fields of cuprate and iron chalcogenide superconducting materials

2019, Buchkov, K., Valkovski, M., Gajda, D., Nenkov, K., Nazarova, E.

The weak links effects are one of the main challenges for effective power applications of high temperature superconducting materials. Studies of these effects help for their better understanding and subsequent improvement. An overview analysis of the intergranular properties of cuprate (Y0.8Ca0.2Ba2Cu3O7-δ) and iron-based chalcogenide (FeSe0.5Te0.5) polycrystalline samples was carried out, by means of series of electro-transport experiments at different magnetic fields. The temperature evolution of the Josephson coupling and intrinsic superconductivity effects for the both systems was constructed. The FeSe0.5Te0.5 compound shows very stable and superior behavior compared to Y0.8Ca0.2BCO up to the highest magnetic fields (14T) used. We have explored FeSe0.5Te0.5 Josephson weak links influence (as a non-linear process) over the resistive transition using different AC current amplitudes and applying the sensitive AC transport third harmonics technique.

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Metrological large range magnetic force microscopy

2018, Dai, G., Hu, X., Sievers, S., Fernández, Scarioni, A., Neu, V., Fluegge, J., Schumacher, H.W.

A new metrological large range magnetic force microscope (Met. LR-MFM) has been developed. In its design, the scanner motion is measured by using three laser interferometers along the x, y, and z axes. Thus, the scanner position and the lift height of the MFM can be accurately and traceably determined with subnanometer accuracy, allowing accurate and traceable MFM measurements. The Met. LR-MFM has a measurement range of 25 mm × 25 mm × 5 mm, larger than conventional MFMs by almost three orders of magnitude. It is capable of measuring samples from the nanoscale to the macroscale, and thus, it has the potential to bridge different magnetic field measurement tools having different spatially resolved scales. Three different measurement strategies referred to as Topo&MFM, MFMXY, and MFMZ have been developed. The Topo&MFM is designed for measuring topography and MFM phase images, similar to conventional MFMs. The MFMXY differs from the Topo&MFM as it does not measure the topography profile of surfaces at the second and successive lines, thus reducing tip wear and saving measurement time. The MFMZ allows the imaging of the stray field in the xz- or yz-planes. A number of measurement examples on a multilayered thin film reference sample made of [Co(0.4 nm)/Pt(0.9 nm)]100 and on a patterned magnetic multilayer [Co(0.4 nm)/Pt(0.9 nm)]10 with stripes with a 9.9 μm line width and 20 μm periodicity are demonstrated, indicating excellent measurement performance.