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- ItemOccurrence of polar mesosphere summer echoes at very high latitudes(München : European Geopyhsical Union, 2009) Zecha, M.; Röttger, J.Observations of polar mesosphere summer echoes (PMSE) have been carried out during the summer periodes 1999–2001 and 2003–2004 at the very high latitude of 78° N using the SOUSY Svalbard Radar (53.5 MHz) at Longyearbyen. Although the measurements could not be done continuously in these seasons, PMSE have been detected over more than 6600 h of 9300 h of observation time overall. Using this data base, particular PMSE occurrence characteristics have been determined. PMSE at Svalbard appear from the middle of May to the end of August with an almost permanent total occurrence in June and July. Diurnal variations are observable in the height-depend occurrence rates and in PMSE thickness, they show a maximum around 09:00–10:00 UTC and a minimum around 21:00–22:00 UTC. PMSE occur nearly exclusively between a height of 80 km and 92 km with a maximum near 85 km. However, PMSE appear not simultaneously over the entire height range, the mean vertical PMSE extension is around 4–6 km in June and July. Furthermore, typically PMSE are separated into several layers, and only 30% of all PMSE are single layers. The probability of multiple layers is greater in June and July than at the beginning and the end of the PMSE season and shows a marked 5-day-variation. The same variation is noticeable in the seasonal dependence of the PMSE occurrence and the PMSE thickness. We finally discuss potential geophysical processes to explain our observational results.
- ItemGas-discharge plasma-assisted functionalization of titanium implant surfaces(Baech : Trans Tech Publications Ltd., 2010) Schröder, Karsten; Finke, Birgit; Polak, Martin; Lüthen, Frank; Nebe, Barbara; Rychly, Joachim; Bader, Rainer; Lukowski, Gerold; Walschus, Uwe; Schlosser, Michael; Ohl, Andreas; Weltmann, Klaus DieterA crucial factor for in-growth of metallic implants in the bone stock is the rapid cellular acceptance whilst prevention of bacterial adhesion on the surface. Such contradictorily adhesion events could be triggered by surface properties. There already exists fundamental knowledge about the influence of physicochemical surface properties like roughness, titanium dioxide modifications, cleanness, and (mainly ceramic) coatings on cell and microbial behavior in vitro and in vivo. The titanium surface can be equipped with antimicrobial properties by plasma-based copper implantation, which allows the release and generation of small concentrations of copper ions during contact with water-based biological liquids. Additionally, the titanium surface was equipped with amino groups by the deposition of an ultrathin plasma polymer. This coating on the one hand does not significantly reduce the generation of copper ions, and on the other hand improves the adhesion and spreading of osteoblast cells. The process development was accompanied by physicochemical surface analyses like XPS, FTIR, contact angle, SEM, and AFM. Very thin modified layers were created, which are resistant to hydrolysis and delamination. These titanium surface functionalizations were found to have either an antimicrobial activity or cell-adhesive properties. Intramuscular implantation of titanium samples coated with the cell-adhesive plasma polymer in rats revealed a reduced inflammation reaction compared to uncoated titanium. © (2010) Trans Tech Publications.
- ItemSupramolecular assemblies of block copolymers as templates for fabrication of nanomaterials(New York, NY [u.a.] : Elsevier, 2011) Nandan, B.; Kuila, B.K.; Stamm, M.Self-assembled polymeric systems have played an important role as templates for nanofabrication; they offer nanotemplates with different morphologies and tunable sizes, are easily removed after reactions, and could be further modified with different functional groups to enhance the interactions. Among the various self-assembled polymeric systems, block copolymer supramolecular assemblies have received considerable attention because of the inherent processing advantages. These supramolecular assemblies are formed by the non-covalent interactions of one of the blocks of the block copolymer with a low molar-mass additive. Selective extraction of the additive leads to porous membranes or nano-objects which could then be used as templates for nanofabrication leading to a variety of ordered organic/inorganic nanostructures. In this feature article, we present an over-view of the recent developments in this area with a special focus on some examples from our group.
- ItemLaser-Induced front Side Etching: An Easy and Fast Method for Sub-μm Structuring of Dielectrics(Amsterdam [u.a.] : Elsevier, 2012) Lorenz, P.; Ehrhardt, M.; Zimmer, K.Laser-induced front side etching (LIFE) is a method for the nanometer-precision structuring of dielectrics, e.g. fused silica, using thin metallic as well as organic absorber layer attached to the laser-irradiated front side of the sample. As laser source an excimer laser with a wavelength of 248 nm and an pulse duration of 25 ns was used. For sub-μm patterning a phase mask illuminated by the top hat laser beam was projected by a Schwarzschild objective. The LIFE process allows the fabrication of well-defined and smooth surface structures with sub-μm lateral etching regions (Δx < 350 nm) and vertical etching depths from 1 nm to sub-mm.
- ItemJosephson and tunneling junctions with thin films of iron based superconductors(Amsterdam [u.a.] : Elsevier, 2012) Schmidt, S.; Döring, S.; Tympel, V.; Schmidl, F.; Haindl, S.; Iida, K.; Holzapfel, B.; Seidel, P.We produced planar hybrid Superconductor - Normal metal - Superconductor (SNS') junctions and interfaceengineered edge junctions (SN'S' or SIS' with normal metal (N') or insulating (I) barrier) with various areas using Co-doped Ba-122 as base electrode. Varying the thickness of the Normal metal (gold) barrier of the planar junctions, we can either observe Josephson behavior at thinner gold thicknesses or transport dominated by Andreev reflection. The edge junctions seem to form a SN'S'-contact.
- ItemCombinatorial synthesis of (YxGd1-x)Ba2Cu3Ox superconducting thin films(Amsterdam [u.a.] : Elsevier, 2012) Kirchner, A.; Erbe, M.; Freudenberg, T.; Hühne, R.; Feys, J.; Van Driessche, I.; Schultz, L.; Holzapfel, B.Environmentally friendly water-based YBa2Cu3Ox (YBCO) and GdBa2Cu3Ox (GdBCO) precursor solutions were synthesized to realize thin films by chemical solution deposition. Pure YBCO and GdBCO precursor solutions were used for ink plotting on SrTiO3 substrates and subsequent thermal treatment at the corresponding crystallization temperature. Phase formation of Gd123 requires a higher crystallization temperature of 840 °C compared to the Y123 phase. The critical temperature of YBCO films is about 92 K with a sharp transition into the superconducting state. Micro liter sized ink volumes of YBCO and GdBCO were successfully mixed for two-dimensional ink plotting of a (YxGd1-x)Ba2Cu3Ox film library. A homogeneous surface and no indication of a-axis growth were found in all mixed films.
- ItemLaser Embossing of Micro-and Submicrometer Surface Structures in Copper(Amsterdam [u.a.] : Elsevier, 2012) Ehrhardt, M.; Lorenz, P.; Frost, F.; Zimmer, K.Micro- and submicrometer structures have been transferred from nickel foils into solid copper surfaces by laser microembossing. The developed arrangement for laser microembossing allows a large-area replication using multi- pulse laser scanning scheme, guaranties a low contamination of the embossed surface and enables the utilization of thick workpieces. In the micrometer range the replicated patterns feature a high accuracy regarding the shape. A significant difference between the master and the replication pattern could be observed for the laser embossing of submicrometer patterns. In conclusion, the results show that the proposed laser embossing process is a promising method with a number of applications in microengineering.
- ItemA superconducting levitation transport model system for dynamical and didactical studies(Amsterdam [u.a.] : Elsevier, 2012) Rosenzweig, St.; Reich, E.; Neu, V.; Berger, D.; Peukert, K.; Holzapfel, B.; Schultz, L.; Pospiech, G.Superconducting levitation transport systems might become very attractive in the near future due to various reasons. The realisation of contactless systems allows e.g. extended maintenance-free operation with high efficiency since such a system only needs energy for cooling and propulsion. We established a small superconducting levitation transport model system called "SupraTrans Mini" consisting of permanent magnetic rails and a levitated vehicle including four YBCO-bulk samples in a cryostat. The rail system consists of an oval shaped loop (2.90 m x 1.44 m), which was build up from individual linear and curved track modules. Inside the vehicle position variations of the superconductors are possible. By means of velocity, acceleration and temperature measurements different dynamical aspects of our complex levitation system can be investigated. We also show the broad applicability of the experimental setup for didactical studies in physics.
- ItemOptimization of the energy deposition in glasses with temporally-shaped femtosecond laser pulses(Amsterdam [u.a.] : Elsevier, 2011) Mauclair, C.; Mishchik, K.; Mermillod-Blondin, A.; Rosenfeld, A.; Hertel, I.V.; Audouard, E.; Stoian, R.Bulk machining of glasses with femtosecond laser pulses enables the fabrication of embedded optical functions. Due to the nonlinear character of the laser-matter interaction, structural modifications can occur within the focal region. To reach a full control of the process, ways of controlling the deposition of the laser energy inside the material have to be unveiled. From static and time-resolved pictures of bulk-excitation of a-SiO2 and borosilicate glass, we show that particular laser temporal shapes such as picosecond sequences can better confine the energy deposition than the femtosecond sequence by reducing the propagation artifacts.
- ItemSuperconductivity in multi-phase Mg-B-O compounds(Amsterdam [u.a.] : Elsevier, 2012) Prikhna, T.; Gawalek, W.; Eisterer, M.; Weber, H.W.; Noudem, J.; Sokolovsky, V.; Chaud, X.; Moshchil, V.; Karpets, M.; Kovylaev, V.; Borimskiy, A.; Tkach, V.; Kozyrev, A.; Kuznietsov, R.; Dellith, J.; Shmidt, C.; Basyuk, T.; Litzkendorf, D.; Karau, F.; Dittrich, U.; Tomsic, M.Structures of MgB2-based materials manufactured under pressure (up to 2 GPa) by different methods having high superconducting performance and connectivity are multiphase and contain different Mg-B-O compounds. Some oxygen can be incorporated into MgB2 and boron into MgO structures, MgBx (X=4-20) inclusions contain practically no oxygen. Regulating manufacturing temperature, pressure, introducing additions one can influence oxygen and boron distribution in the materials and thus, affect the formation, amount and sizes of Mg-B-O and MgBx inclusions and changing type of pinning, pinning force and so affect critical current density jc. The boron concentration increase in initial Mg and B mixture allows obtaining sample containing 88.5 wt% of MgB12 with Tc of 37.4 K (estimated magnetically).